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a new method for determining the crack closure stress (cc) and crack initiation stress (ci) from laboratory data is presented and compared with other methods. a new method called continuous strain deviation (csd) is proposed and applied to determine cc and ci. the csd method is based on the fact that there are usually subtle changes in the stress-strain curve which could be due to the crack closure or initiation. starting from an initial point corresponding to 30% to 40% ucs, the proposed algorithm provides a distinct indicator for cc and ci. the cc and ci for badaling granite and sp diorite are determined with the proposed method, results from which are similar to other methods. sensitivity analyses of the csd method show that stable cc and ci values could be estimated using any initial point from 30% to 40% ucs. the comparison studies show that the csd method predicts a smaller stress range and gives a more distinct indicator for both cc and ci.

in this study, the microstructure and pore-scale damage mechanisms of a novel, stable type of microgel (mg) used in oil-based nanocomposite applications are characterized. the mg consists of hydrophobic silica particles capped with hydrophobic chains of poly(n-butyl methacrylate) (pnbma). the formation of the microgel is influenced by the surface functionality of the silica and by the polymer template in the oil phase. a systematic method for synthesizing the mg was developed, and the mg-based nanocomposite was characterized. the average pore size of the mg is smaller than that of the mg precursor, indicating that a densification process occurred during the microgel synthesis process. the pore-wall microstructure and pore-scale damage mechanisms of the mg were characterized by examining the uniaxial compressive and unconfined compressive stress-strain curves of the mg-based nanocomposite. the compressive modulus of the mg-based nanocomposite is only 25% of the modulus of the mg precursor. this is attributed to the densification of the mg. the compressive strength of the mg-based nanocomposite was evaluated by unconfined compression tests and the results show that the compressive strength of the mg-based nanocomposite is ∼30% of the compressive strength of the mg precursor. this is due to the fact that the mg particle has a larger area of contact with the matrix than does the mg precursor. in addition, the mg-based nanocomposite is much more brittle than the mg precursor.

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